epa method 7471

Aqueous samples are digested with sulfuric acid, nitric acid, potassium permanganate, and potassium persulfate in order to oxidize the organo-mercury compounds to the mercuric ion. sand, silica gel, acid binder, universal binder, sawdust). Method 3015, Revision 0 (1994) (PDF) (10 pp, 329 Kb) MICROWAVE ASSISTED ACID DIGESTION OF AQUEOUS SAMPLES AND EXTRACTS. United States Environmental Protection Agency, You may need a PDF reader to view some of the files on this page. endobj 1000 Series. STABILITY AND REACTIVITY ��0��i�)~�Ε ��%��]"h3��g�s�C�x�u ��*�zܜd�F}(oٰ̾��x�5�e��a�@,)��IP\? Partition coefficient (n-octanol/water): Not available. The quantitation limit will depend on the volume of sample used to trap the mercury by the use of gold. This is possible by inserting a gold trap in the CV AAS technique to amalgamate the Hgº vapor formed and heat it to volatilize mercury for analysis. See EPA’s About PDF page to learn more. An official website of the United States government. Laboratory Method … The protocols for Methods 7470 and 7471 in the SW-846 methods manual are designed for the cold-vapor atomic absorption spectrometric (CV-AAS) determination of total mercury in aqueous (extracts, wastewater, ground water, etc.) Highlighted Resources. 2 0 obj If this dissolution procedure is not sufficient to dissolve a specific matrix type or sample, then this method is not applicable for that matrix. <> 7.2 See Method 7000, Paragraph 7.3, Furnace Procedure. 1 0 obj concentrations), Target Analyte List (TAL Metals) by EPA Methods 6010B/7471 S-2 12/5/2006 12/5/2006 Soil Soil boring using hand auger Hand auger 1 2-2.5 PCBs via EPA method 8082, TPH via EPA method 8015M (with fingerprint analysis performed on detectable concentrations), VOCs by EPA Method 8260B, and SVOCs by EPA Method 8270 (PAHs only) S-3 12/5/2006 12/5/2006 Soil Soil boring using hand … Decomposition temperature: Not available. 6000 Series. x��[K�۸��f�|��v�qŕ��'�T��Ę"��Y�קRR3I�� (4��u�ט(��F?�/��~�e��_^��8�b�E��^��}��(��b�/�g��W7�t��៯_%QP��oް;��?Pʴ(��V�F(��H�E�"HP��i��bӏ�?�8T[fk��\�p��Y�z�*͂�0;ݝ+ ��z��%��=�x��؂zH�`�_� The language in the method was revised for Method 7471B (in Update IVA), where Sec. 2.2 This method uses cold-vapor atomic absorption and is based on the absorption of radiation at the 253.7-nm wavelength by mercury vapor. Validated Methods. EPA SW-846, Test Methods for Evaluating Solid Wute, 3rd Edition, Nov. 1986 USEPA Contract Laboratory Program, Statement of Work for Organics Analysis, Multi-Media, Multi-Concentration (3) Methods for Chemical Analysis of Water and Wutes EPA-600/4-79-020 Revised March 1983 (4) BCM Inc. 9.0 METHOD PERFORMANCE 9.1 Precision and accuracy data are not available at this time. 9.2 The performance characteristics for an aqueous sample free of interferences are: Optimum concentration range: 5-100 … %�� The HotBlocks can maintain a temperature of ambient+5°C up to 150°C. ?�w��JuŤ;N��:��FH#XdׂF9��{��؎�8r�{��뽨/�:+��h�vl�t�p��j�ю}W�j쭚V9��(%�V'K�4&;�k�b�wU�ܹ�u�$03��C��#��:�.^vMu�ȏж׮ʇ�P��od��t��]��F];F�k��킾��̫��=u�C�A41(��, Vw�=��` �Q4�� {�9�c��B}9B��hv\��0L��j[S�@�H#��E��6�܀�x��u�6\��2^�ѵWl�� Hu�?.��|+�Mj��Nr�K��WȑK�g@�-��4 �1E�s��}7��:��ƛ�v�7�֨r��~C�Mt*d��)5V��&Y��Bu[p{��:��'[�g�9��7K磹��GQ�W��L��c�� wAπ�$�O?��7�-�vs4Q��f��M�>�j;��"��bWفz)�qbʡW �d�:v��!��9�|H�,.E�� c]r�� Џ��7�X��\7��L]�Pt�v��ݯ�w[�ٳB�LNi6�5�ǘv?��d�I��, ��J��i/��w��?|��J��r1[F��=?��ϭ0f̨s�N��쑏��t�_�;�~\�z��|y�� Y�'SOG�{�IfVQ�X��,�\%�u��J�=z:�n>�QN�cCi�O�Y��C. 2. <>>>/TrimBox[0 0 612 792]/MediaBox[0 0 612 792]>> 7.2 See Method 7000, Paragraph 7.3, Furnace Procedure. METHOD 7471 MERCURY IN SOLID OR SEMISOLID WASTE (MANUAL COLD-VAPOR TECHNIQUE) 1.0 SCOPE AND APPLICATION 1.1 Method 7471 1s approved for measuring total mercury (organic and inorganic) in soils, sediments, bottom deposits, and sludge-type materials. Gebhart, J. D. Messman, and G. F. Wallace The EPA … 2.2 Method 7471, a cold-vapor atomic absorption method, is based on the absorption of radiation at the 253.7-nm wavelength by mercury vapor. 8.0 QUALITY CONTROL 8.1 See Section 8.0 of Method 7000. To find out if Summit conducts this test, contact us at 330-253-8211 today. See EPA’s, Selected Analytical Methods for Environmental Remediation and Recovery (SAM), Method 7471B: Mercury in Solid or Semisolid Waste (Manual Cold-Vapor Technique), part of Test Methods for Evaluating Solid Waste, Physical/Chemical Methods (PDF), Sample Collection Information Documents (SCIDs), Sample Collection Procedures and Strategies. 7471B - 2 Revision 2 February 2007 2.0 SUMMARY OF METHOD 2.1 Prior to analysis, the solid or semi-solid samples must be prepared according to the procedures discussed in this method. The mercury is reduced to the elemental state and aerated from solution in a closed system. Gaskill, A., Compilation and Evaluation of RCRA Method Performance Data, Work Assignment No. Utilizing Cold Vapor Atomic Absorption (CVAA) technology, total mercury analysis is suitable for a variety of matrices including waters, soils, sediments and wastes. materials, respectively. Primarily for the purpose of monitoring for mercury levels in fish and in support of consumption advisories, many environmental laboratories routinely utilize a common testing method, EPA Method 7471A: Mercury in Solid or Semisolid Waste(EPA 7471), for the preparation and analyses of biota samples for total mercury concentrations. EPA’s Selected Analytical Methods for Environmental Remediation and Recovery (SAM) lists this method for preparation and/or analysis of solid and wipe samples for mercury, mercuric chloride (analyzed as total mercury), and methoxyethylmercuric acetate (analyzed as total mercury). This document is included in Selected Analytical Methods for Environmental Remediation and Recovery (SAM). Product name: LOCTITE SF 7471 PRIMER known as LOCTITE® 7471™ Primer LOCQUIC® Page 4 of 6 Solubility in water: Not available. We believe that the text in Method 7471A specified triplicate weighings in order to achieve a more homogeneous subsample of the original field sample. The calculation is given in Method 7000, Paragraph 7.4. EPA Method 200.7 uses ICP-OES for regulatory compliance for drinking water analysis. Main menu . 9.2 The performance characteristics for an aqueous sample free of … Contact Us to ask a question, provide feedback, or report a problem. %PDF-1.3 View Actual EPA Method 7471B (PDF File) All samples must be subjected to an appropriate dissolution step prior to analysis. The information contained in this method is provided by EPA as guidance to be used by the analyst and the regulated community in making judgments necessary to generate results that meet the data quality objectives for the intended application. What is the temperature range on the SC100 Hotblock? The information contained in this method is provided by EPA as guidance to be used by the analyst and the regulated community in making judgments necessary to generate results that meet the data quality objectives for the intended application. 9000 Series. MERCURY IN LIQUID WASTE (MANUAL COLD-VAPOR TECHNIQUE).0 SCOPE AND APPLICATION 1.1 Method 7470 is a cold-vapor atomic absorption procedure approved for determining the concentration of mercury in mobility-procedure extracts, aque- ous wastes, and ground waters. 7000 Series. Product name: LOCTITE SF 7471 PRIMER known as Loctite(R) 7471 Primer T Page 3 of 6 Clean-up methods: Remove all sources of ignition. Method 7471B: Mercury in Solid or Semisolid Waste (Manual Cold-Vapor Technique), part of Test Methods for Evaluating Solid Waste, Physical/Chemical Methods (PDF) (11 pp, 1 MB, February 2007) Contact Us to ask a question, provide feedback, or report a problem. Air; Bed Bugs; Chemicals and … 5000 Series. 2, EPA Contract No. The only thing to be aware of is differences in volume. Screening Level 14 (µg/kg dry weight) [Minimum Detection Limit must be lower]: Total polychlorinated biphenyls (PCB) Footnote 15 Footnote 16 MA400-BPC 1.0 or EPA 1668C 17: method and/or lab dependent: 100: Total polycyclic aromatic hydrocarbons (PAH) Footnote 15 Footnote 18 EPA 8270C Environmental Topics. 11.1 (in the EMMC format) directs the user to weigh out 0.5 to 0.6 g of a well-homogenized sample. All of the documents found in the Third Edition of SW-846, as updated by Updates I, II, IIA, IIB, III, IIIA, IIIB, IVA and IVB are located at this site. Generally speaking, the same digestion times and temperatures will apply as given in each method. Metals were analyzed in the residue by EPA Method 6010 except for mercury which was analyzed by EPA Method 7471. 4000 Series . Methodologies include NELAP approved EPA Method 200.7, EPA SW-846 Method 6010 for ICP metals and EPA Method 245.1, EPA SW-846 Method 7470/7471 for Mercury analyses. Method 1631E has a quantitation level of 0.5 ppt, making it 400 times more sensitive than Methods 245.1 and 245.2. <>stream ----- PB88-196001 EPA/600/4-88/011 April 1988 INTERLABORATORY EVALUATION OF SW-846 METHODS 7470 AND 7471 FOR THE DETERMINATION OF MERCURY IN ENVIRONMENTAL SAMPLES by J. E. Gebhart, J. D. Messman, and G. F. Wallace Battelle Columbus Division Columbus, Ohio 43201-2693 Contract Number 68-03-3226 Work Assignment 1-12 Project Officer WERNER F. BECKERT QUALITY ASSURANCE AND METHODS … See EPA's PDF page to learn more. 68-01-7075, September 1986. You can email us at info@envexp.com. 9.0 METHOD PERFORMANCE 9.1 Precision and accuracy data are available in Method 239.2 of Method s for Chemical Analysis of Water and Wastes. All samples must be subjected to an appropriate dissolution step prior to analysis. Organics: Analytical Method Footnote 12: Target 13 Detection Limit (mg/kg dry weight). We just received a new hotblock. Total Mercury Analysis (EPA SW-846 Method 7471/7470) Total mercury analysis is the most routine mercury testing procedure performed. Additionally, EPA approved Method 1631 Revision E in 2002. Soak up with inert absorbent material (e.g. EPA’s Selected Analytical Methods for Environmental Remediation and Recovery (SAM) lists this method for use if problems occur when using EPA Method 7473 during preparation and analysis of solid and wipe samples containing mercury, mercuric chloride (analyzed as total mercury), and methoxyethylmercuric acetate (analyzed as total mercury). Referred Air Methods. and solid (soils, sediments, sludges, etc.) SW-846 Online: Test Methods for Evaluating Solid Waste, Physical/Chemical Methods Brief Method Summary. Our HotBlock manuals come with adapted versions of several EPA methods including 200.2, 200.7, 200.8, 245.1, 7470, 7471, 365.2, 3050B, and NIOSH method 7303. endobj The mercury vapor passes through a cell positioned in the light path of an atomic absorption spectrophotometer. You may need a PDF reader to view some of the files on this page. Wear appropriate personal protective equipment. EPA 3050B: EPA 7470: EPA 7471: Don't see your test method listed? 8000 Series. Methods for Chemical Analysis of Water and Wastes, EPA-600/4-82-055, December 1982, Method 213.1. United States Environmental Protection Agency Environmental Monitoring Systems Laboratory Las Vegas, NV 89193-3478 Research and Development EPA/600/S4-88/011 August 1988 v>EPA Project Summary Interlaboratory Evaluation of SW-846 Methods 7470 and 7471 for the Determination of Mercury in Environmental Samples Werner F. Beckert, J.E. The calculation is given in Method 7000, Paragraph 7.4. Method 7471B: Mercury in Solid or Semisolid Waste (Manual Cold-Vapor Technique), part of Test Methods for Evaluating Solid Waste, Physical/Chemical Methods (PDF) (11 pp, 1 MB, February 2007) Contact Us to ask a question, provide feedback, or report a problem. 3000 Series. 10. 8.0 QUALITY CONTROL 8.1 See Section 8.0 of Method 7000. Method 7471 is approved for measuring total mercury (organic and inorganic) in soils, sediments, bottom deposits, and sludge-type materials. Table of Contents. See EPA’s About PDF page to learn more. SW-846 contains over 200 documents, including the Table of Contents, Disclaimer, Preface, Chapters One through Thirteen, and many different methods for the sampling and analysis of wastes. Method 6010 was developed for RCRA regulations and the method cannot be used for regulatory compliance monitoring for Safe Drinking Water Act and Clean Water Act. EPA Method 7471B (SW-846): Mercury in Solid or Semisolid Wastes (Manual Cold-Vapor Technique) This document is included in Selected Analytical Methods for Environmental Remediation and … Keep unnecessary personnel away. Posts Tagged ‘EPA Method 7471’ Analytical Techniques for MACT Industrial Boilers Emissions Standards Sunday, February 5th, 2006 On September 13, 2004, the EPA promulgated Maximum Achievable Control Technology (MACT) emissions standards for industrial boilers. EPA Method 7471B Summit Environmental Technologies prides itself in its expansive testing capabilities in a variety of different fields. Question/Answer . EPA-RCA Citation. Ensure adequate ventilation. EPA Method 624 plus xylenes, 1 ppb detection limits for volatile organic compounds . VOC content: 13.3 %; 106 g/l EPA Method 24 Viscosity: Not available. Do you have a specification sheet available? 3 0 obj If you are EPA Method 7470A (SW-846): Mercury in Liquid Wastes (Manual Cold-Vapor Technique) This document is included in Selected Analytical Methods for Environmental Remediation and Recovery (SAM). The method can also be used for analysis of other matrices, such as wastewater, groundwater, soil, sediments, and solid waste. 1.4 Use of this method is restricted to use by, or under supervision of, properly analysts experienced and trained in the analysis of trace elements at very low concentrations The heat content (higher heating value, HHV), as well as, moisture, ash, carbon, hydrogen, oxygen, nitrogen, and sulfur contents of both the firelogs and their combustion residues were determined by proximate/ultimate analyses. Modification of US EPA 7470A/7471A (US EPA, 2009p; 2009q) methods permits lower quantitation limits for mercury. (EPA/SW-846 Methods 7000A/7470A/7471A) CONTENTS 1.0 SCOPE AND APPLICATION* 2.0 METHOD SUMMARY 3.0 SAMPLE PRESERVATION, CONTAINERS, HANDLING, AND STORAGE 4.0 INTERFERENCES AND POTENTIAL PROBLEMS 5.0 EQUIPMENT/APPARATUS 6.0 REAGENTS* 7.0 PROCEDURES 7.1 Glassware Preparation 7.2 Total Solids 7.3 Sample Preparation 7.3.1 Soil, Sediment, Solid, and … Chapters. Once the digested samples have cooled, sodium chloride-hydroxylamine sulfate is added … 0010 - 0100 Series. Method … Please let us know. Accuracy data are not available 7470: EPA 7471: Do n't See your test Method?. Environmental Protection Agency, you may need a PDF reader to view some of the original field sample solid soils... 0.5 ppt, making it 400 times more sensitive than Methods 245.1 and 245.2 624 plus xylenes, 1 detection! Data are available in Method 7000, Paragraph 7.3, Furnace Procedure provide... 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